Solid perfume mixture containing artificial musk.



with one or several ethereal oils, melting the whole, and casting themass into suitable No Drawing.

UNITED STATES PATENT OFFICE.

ALEXANDERST'AP'LER, CHABLQTTENBURG, GERMANY.

SOLID PERFUME MI [XTURE CONTAINING. ARTIFICIAL MUSK.

Specification of Letters Patent. Patented Aug, 15, 1911, Applicationfiled September 22, 1909. Serial No. 519,083.

Solid Perfume Mixture Containing Artificial Musk, of which the followingis a full,

clear, and exact description.

.Combinatiens of perfumes insolid form may be obtained by mixingartificial musk molds. In this manner combinations of perfumes areobtained in' aconvenient form, such'for instance as cartridge or pencilform, or in any other desired shape.

According to the class of ethereal oils chosen and combined with themusk a great variety of diflerent odors will be'obtained. Thesecombinations will consist solely of perfumes, and not as is the-casewith the perfumes in solid form heretofore known of an ineffective massor carrying medium impregnated or mixed wlthperfume, which 15 notodorous and soon loses by evaporation the comparatively small amount ofper fume with which it was impregnated. On

an increase of temperature, the combinations attained by the present invntion retain their odorfor a very long time even in high summertemperatures, in which they do not melt as do the customary perfumes,but remain solid.

The invention may be carried out for instance in the. following manner:165 gr. of artificial musk containing acetanilid are melted and allowedto solidify, and 50 gr. of

pure ethereal voil for instance the so-called artificial oil of liliesof the yalley, or oils of similar suitable properties are mixedtherewith, the mixture melted by the application of heat,'and the wholemass then cast into molds. Or, 165' gr. of'musk Baurand .65 gr. ofheliotropin or 65 gr. of cumarin are well mixed with gr. of a pureethereal (not fatty) flower oil, for instance the socalled artificialoil of lilies-of-the-yalley, the

mixture melted by the application of heat,

and is then cast into molds. The combinations of perfumes attained inthis manner in solid form, consist of perfectly homo geneous massesj Iclaim 1. As a new article of manufacture, a solid perfume, the samecomprising the product ethereal oil, substantially as described.

3. As a new article of manufacture, a

solid perfume, the same comprising the" product resulting from thefusing together ofartificial musk containing aeetanilid and anotherperfume comprising the so-called artificial oil of lilies-of-the-valley,substantially as described.

4. As a new article of manufacture, a solid perfume, the same consistingof the product resulting from the fusingtogether of artificial muskcontaining acetanilid, a

fragrant ethereal on, and another, perfume, substantially as described.

5. As a new article of manufacture, a solid perfume, the same consistingof the product resulting from the fusing together of artificial muskcontaining acetanilid, a fragrant ethereal oil, and another perfume, inthe proportions of 165 parts of said artificial musk containingacetanilid, 50 parts of said fragrant oil, and '65 parts of saidperfume, substantially as described.

6. As a new article of manufacture, a

.solid perfume,,the same consisting of the product resulting from thefusing together of artificial musk containing acetanilid, the

so called artificial oil of ,lilies-of-the-valley, and heliotropin,substantially as described.

7. As a new article ofmanufactfire, a solid perfume, the sameconsisting" of the product resulting from the fusing together ofartificial musk containing acetanilid, the so-called artificial oil oflilies-of-the-valley, and heliotropin, in the proportions of 165 partsof said artificial musk containing acetanilid, 50 parts of said oiloflilies-of-thevalley, and 65 parts of said heliotropin, substantially asdescribed.

8. The hereindescribed process for the manufacture of a solidperfume,which consists in mixing artificial musk containing acetanilid withanotherjserfume comprising afragrant ethereal oil, melting the mixtureby the application of heat, pouring the mix- 7 sists in mixingartificial musk containing acetanilid with another perfume comprisingthe so-called artificial oil of lilies-of-thevalley, melting the mixtureby the application of heat, pouring the mixture into suitable molds, andallowing it to solidify in the desired shape.

10. The hereindescribed process for the manufacture of a solidperfume,'which con sists in mixing artificial musk containingac'etanilid with a fra rant ethereal oil and another perfume, me tingthe mixture by the application of heat, pouring the mixture intosuitable molds, and allowing itto solidify in the desired shape. r

11. The hereindescribed process for the manufacture of a solid perfume,which consists in mixing artificial musk containing acet-anilid with theso-called artificial oil of lilie's-of-the-v'alley and heliotropin,melting the mixture by the application of heat, pouring the mixture intosuitable molds, and allowing it to solidify in the desired shape.

12. The "hereindescribed process for the manufacture of a solid perfume,which consists in mixing 165 parts artificial musk containing acetanilidwith 50 parts 0f the socalled artificial oil ofliIiesOf-the-Valley and65 parts of heliotropin, melting the mixture by the application of heat,pouring the mixture into suitable molds, and allowing it to solidify inthe desired shape.

In testimony whereof I aflix my signature in the presence-0f twowitnesses.

ALEXANDER STAPLER. Witnessesz- HENRY HAsPER, WOLDEMAR HAUPT.

